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Yayın Thermal quenching of thermoluminescence in quartz samples of various origins(Univ Agean, Dept Mediterranean Stud, 2010) Subedi, Bhagawan; Afouxenidis, Dimitrios; Polymeris, George S.; Bakoglidis, Konstantinos D.; Raptis, Spyridoula; Tsirliganis, Nestor C.; Kitis, GeorgeThe effect of thermal quenching plays an important role in the thermoluminescence (TL) of quartz on which many applications of TL are based. In present work it is investigated that the thermal quenching parameters i.e. the activation energy W and the dimensionless parameter C, are more or less the same for every kind of quartzes or sample dependent on strong external treatment like a high temperature annealing. This preliminary investigation of seven quartz samples of different origin showed that the thermal quenching parameters W and C are common (universal) for most of the quartz samples.Yayın Preliminary TL and OSL investigations of obsidian samples(Univ Agean, Dept Mediterranean Stud, 2010) Polymeris, George S.; Gogou, D.; Afouxenidis, Dimitrios; Rapti, Sofia; Tsirliganis, Nestor C.; Kitis, GeorgeObsidian is a volcaniclastic mineral extremely hard to break, which was used in prehistoric Greece (and elsewhere in the World), in order to provide tools, weapons, knives and arrowheads. The present work aims to characterize this extremely precious tool stone by using both thermoluminescence (TL) and optically stimulated luminescence (OSL) techniques and investigate its potential use for luminescence dating purposes. Basic TL and OSL properties, such as TL and OSL thermal and optical stability, repeatability, TL and LM-OSL glow curve shape and mainly the linearity of the TL and OSL signals as a function of beta dose were investigated. Artificially irradiated samples indicate all promising luminescence features, such as the 110 degrees C TL peak and dose response sub-linearity for intermediate doses, quick and effective bleaching all over the entire TL glow curve, along with quite linear CW-OSL dose response for doses larger than 5 Gy. The lack of predose sensitisation indicates the suitability of the material for single aliquot measurements. Furthermore, several features provide indications that the signal does not relate to quartz, but in fact to other silicates. Unfortunately, both lack of bleaching ability for NIL signal, along with a peculiar shape of NOSL, provide major difficulties in dating applications.Yayın A comparative morphological, compositional and tl study of tenedos (Bozcaada) and Sile aeolianites, Turkey(Univ Agean, 2012) Polymeris, George S.; Erginal, Ahmet Evren; Güneç Kıyak, NafiyeAeolianites are carbonate-cemented deposits of coastal dune sands, mostly of Quaternary age. Even though aeolianite exposures on the coasts of the Mediterranean Sea are frequent, very few records have been documented from the coasts of either the Aegean or the Black Sea. The present study deals with evaluating and comparing both compositions and thermoluminescence (TL) ages of two recently reported samples of coastal aeolianites. Both were recovered at the Turkish coasts of Tenedos (Bozcaada) island, Aegean Sea and Şile, Western Black Sea. In the latter case, being the first record for the specific coastal area, the oldest age obtained was dated at 158±25 ka while the youngest age yielded was 108±14 ka. These values imply that both deposition and cementation occurred during the high sea stand of marine isotope stage 5 (MIS 5). In the case of Tenedos, the aeolianites were deposited between the early stage of the oxygen isotope stage 2 period (OIS 2) and the very late phase of the oxygen isotope stage 3 period (OIS 3). These latter TL results are in excellent agreement with a previous study of the same complex after applying OSL. Besides the ages, a number of luminescent features and properties in conjunction with compositional data suggest the dissimilarity for the quartz samples extracted from the aeolianites recovered at these two sampling sites, excluding thus any transport from one sampling site to the other, despite the short distance of the two sampling sites and the meteorological data regarding the preferable wind directions between them.Yayın The firing temperature of pottery from ancient Mesopotamia, Turkey, using luminescence methods: a case study for different grain-size fractions(Wiley-Blackwell, 2014-10) Polymeris, George S.; Güneç Kıyak, Nafiye; Koul, Dileep K.; Kitis, GeorgeThe assessment of the firing temperature of a prehistoric pottery sample collected from ancient Mesopotamia, Turkey was studied using luminescence techniques. The methods for this estimation involved the observation of the thermal and pre-dose sensitization with various re-firing temperatures for both TL and the OSL signals. In the former case, the 110 degrees C TL peak and the rest of the glow curve were used as proxies in this study. In the framework of a first attempt to investigate the impact of grain-size dependence on the sensitization of the luminescence signals, the aforementioned study was performed with four different pottery grain-size fractions: (i) less than 60m, (ii) 60-90m, (iii) 90-180m and (iv) 180-250m. The results clearly demonstrated the firing temperature mark of approximate to 500 degrees C in for the grain size of 90-180m, whileas in the case of the lower grain-size fractiona third proxy, the ratio of the pre-dosed to the thermal sensitization, was seen to indicate the firing temperature. The remaining two grain-size fractions failed to provide any meaningful results with regard to the firing temperature estimation. The dependence of the TL characteristics on the grain size was explained in the framework of the mixed mineralogy.Yayın New quartz technique for OSL dating of limestones(2010) Liritzis, Ioannis; Drivaliari, N.; Polymeris, George S.; Katagas, Christos G.The equivalent dose De determination of limestone-made ancient constructions by thermoluminescence (TL) prevents accurate measurements and requires plateau test of bleached curves. Optical stimulated luminescence (OSL) of quartz and feldspar minerals for surface dating is routinely applied for De but not for limestones. Here the OSL of present traces of such minerals removed with powder from surface limestone bleached by sunlight overcomes this issue and offers an alternative way for De. This is verified with further test examples.Yayın Luminescence dating of prehistoric site of smintheion (Gulpinar) in NW Turkey(Univ Agean, Dept Mediterranean Stud, 2010) Güneç Kıyak, Nafiye; Takaoğlu, Turan; Erginal, Ahmet Evren; Özcan, HalilThis study aims to place the prehistoric settlement of Smintheion in northwestern Turkey in its temporal setting on the basis of the dating of the quartz from pottery and sediments collected from the site employing Optically Stimulated Luminescence and Thermoluminescence techniques. The site belongs to the problematic Middle Chalcolithic period in western Anatolia. This period represents a cultural upheaval in western Anatolia as it has a completely different material culture when compared to that of the preceding Early Chalcolithic period. The pottery and sediment samples were collected from two different locations of the Middle Chalcolithic settlement at Smintheion for dating study. The fact that this examined settlement is represented by a single cultural level provides an opportunity to obtain secure and reliable dates for the settlement. Results of this study show that the site can be dated to a period between 4800 and 4500 B.C.Yayın Investigation of the OSL signal from very deep traps in natural quartz(Univ Agean, Dept Mediterranean Stud, 2010) Kitis, George; Güneç Kıyak, Nafiye; Polymeris, George S.; Pagonis, VasilisIt has been recently reported by several studies that a thermally transferred optically stimulated luminescence (TT-OSL) signal from quartz grains can be used to extend the dating range for quartz samples. The TT-OSL signals are believed to consist of a recuperated OSL (ReOSL) component and a basic-transferred OSL (BT-OSL) component. In the present work the TT-OSL signals from several types of unfired quartz samples were studied. A special protocol was used, which allowed the measure the OSL from very deep traps (VDT) as a function of the OSL stimulation temperature. It was found that all quartz samples exhibit TT-OSL signals, which are depended on sample and on the OSL stimulation temperature. The activation energy of the process was evaluated and the influences of the TT-OSL on the ReOSL dating protocol are discussed.
